2,4-Di-tert-butylphenol explained

2,4-Di-tert-butylphenol (2,4-DTBP) is a white solid with a phenolic odour. It is primarily used as a raw material for the production of several commercially important antioxidants and phenolic benzotriazole-type UV absorbers. It also finds use as a starting material in the synthesis of agrochemicals, fragrances and catalysts (i.e. Jacobsen's catalyst).

Synthesis

The butylation of phenol is typically achieved by a Friedel-Crafts alkylation with isobutylene catalysed by a strong acid. These acids can be either liquids like triflic acid, or solid acids such as zeolites. The isobutylene can be generated in situ by the dehydration of tert-butyl alcohol or methyl tert-butyl ether, which being liquids are simpler to handle than the highly flammable isobutylene gas.[1]

Applications

2,4-DTBP is used in the production of antioxidants like tris(2,4-di-tert-butylphenyl)phosphite.

See also

Notes and References

  1. Yadav . Ganapati D . Doshi . Nirav S . Alkylation of phenol with methyl-tert-butyl ether and tert-butanol over solid acids: efficacies of clay-based catalysts . Applied Catalysis A: General . September 2002 . 236 . 1–2 . 129–147 . 10.1016/S0926-860X(02)00300-9.